My first run on my first still

Directions

  1. 1Perform a vinegar and water cleaning run for 4 hours.
  2. 2Set up the still with an Anvil Foundry 6.5 gallon boiler and an Aliexpress 2" stainless reflux still, including a 200 mm dephlegmator, 400 mm shotgun condenser, sight glass, and a 500 mm tall extension packed with stainless steel scrubbers and copper mesh.
  3. 3Load the boiler with 19 liters (5 gallons) of birdwatchers 10.1% ABV wash.
  4. 4Turn on the boiling with a 120 volt/1600 watt element at 100% power.
  5. 5After about 30 minutes, turn on the water pump for the 65-liter recycling water cooling tank with two frozen 3.7L/1 gallon water jugs.
  6. 6Open the water valve 100% to the dephlegmator but keep it closed for the product condenser.
  7. 7Allow the top column temperature to reach 60C/140F in approximately 30-45 minutes.
  8. 8Open the valve for the product condenser to 100%.
  9. 9After about another 30 minutes, begin collecting fore shots (100 ml, light blue/green, smelling of methanol).
  10. 10After collecting Jar #1, reduce the power to 90% and turn the water valve for the dephlegmator down to 80%, keeping water flow to the product condenser at 100% for most of the run.
  11. 11Every 30 minutes, turn the dephlegmator water valve up to 100% until the column temp drops 1-2 C, then close it back down to 80% to observe reflux.
  12. 12Monitor the spirit coming off the product condenser at 24-25C/76-78F, collecting it as constant drops/broken stream.
  13. 13Change ice jugs in the water tank once during the run as the temperature rises.
  14. 14Shut down the still when the boiler temperature reaches 100C/212F and the product begins to smell like tomato paste.
  15. 15Take a 25 ml sample from the start of Jar #3 and proof it down to 40% ABV for testing.

Ingredients

  • 19 liter birdwatchers 10.1% ABV wash
  • vinegar and water
  • 100 ml Fore Shot
  • 400 ml Jar #1
  • 350 ml Jar #2
  • 600 ml Jar #3
  • 225 ml Jar #4
  • 25 ml sample from the start of jar #3
  • 19 liter birdwatchers 11% ABV batch

Equipment

Anvil Foundry 6.5 gallon boilerAliexpress 2" stainless reflux still200 mm dephlegmator400 mm shotgun condensersight glass500 mm tall extension packed with alternating 100% stainless steel scrubbers and 100% pure copper meshwater pump65 liter recycling water cooling tankfrozen 3.7L/1 gallon water jugs120 volt/1600 watt elementgraduated cylinderpond pump (1000 lph/264 gph)13 mm/1/2 inch T fitting5 mm ID/8 mm OD linesneedle valvesdigital thermometertemp probessimple/radiator fan setup with soft copper line loop on a box fan

Tips

  • Take better notes during the run with times, temps, and settings.
  • Get smaller cuts jars (around 250 ml) for more precise cuts.
  • Consider adjustments to the cooling system, potentially adding another pond pump for the dephleg or a radiator fan setup.
  • Concentrate on takeoff speeds and cuts, rather than solely relying on temperature readings.
  • Get familiar with the smells and tastes of your runs.
  • Avoid tinkering with the reflux condenser (RC) water mid-run; find a balance of water vs. power and stick to it.
  • Maintain a constant water temperature.
  • Consider adding another 500mm packed column with insulation for better separation.
  • Be careful not to rush heating up to avoid puking and scorching, especially without anti-foaming agents or proper degassing.